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Supplementary material for Journal of Materials

supplementary material for journal of materials chemistry this journal is © the royal society of chemistry 2002 supplementary m
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Supplementary material for Journal of Materials Chemistry
This journal is © The Royal Society of Chemistry 2002
SUPPLEMENTARY MATERIAL
Fluorescence and Physical Characterization of SolGelDerived
Nanocomposite Films Suitable for the Entrapment of Biomolecules
Gillian Goring and John D. Brennan*
Department of Chemistry, McMaster University, Hamilton, Ontario, L8S
4M1, Canada
Table S1. Gelation time of silane mixtures used to produce thin films.
Silane composition
pH 4.00a
TRIS/Phos
pH 5.50a
TRIS/Phos
pH 7.26a
TRIS/Phos
pH 8.5a
TRIS/Phos
pH 10a
TRIS/Phos
TEOSb
>24 hr/24hr+
>24 hr /16hr
160minb/4.5min
5.0min/4.0min
3.0min/2.0min
10% MTES
>24 hr/>24 hr
>24 hr/>24 hr
>24 hr/11.0min
13.0min/8.0min
6.0min/8.5min
20% MTESb
>24 hr/>24 hr
>24 hr/>24 hr
120minb/31min
32min/16min
13.5min/13min
40% MTES
>24 hr/>24 hr
>24 hr/>24 hr
>24 hr/60min
120min/30min
25min/40min
2% DMDMS
>24 hr/>24 hr
>24 hr/>24 hr
>24 hr/8.0min
5.5min/3.0min
3.0min/3.5min
10% DMDMSb
>24 hr/>24 hr
>24 hr/18hr
90minb/4.0min
11.0min/3.0min
5.5min/24 hr/>24 hr
>24 hr/>24 hr
>24 hr/6.0min
7.0min/5.0min
4.0min/4.0min
a Errors on the pH range: pH 4.00  0.05; pH 5.50  0.10; pH 7.26 
0.03; pH 8.50  0.10;
pH 10.00  0.05, TRIS is tris buffer, Phos is phosphate buffer
b Boldface values show the compositions used to form the films that
were studied in this paper.

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